DT275

Module 2 Assignments

 

 

There are two assignments for this module.  Assignment 1 is on heat transfer.  Assignment 2 is on fluid flow.  There are 25 marks for each assignment and 50 marks for the exam.

Note that a defence of your work at interview may be requested to assist in the assessment of all assignments.

 

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Module 2 Assignment 1

Heat Transfer

 

Lecturer: paul.ashall@dit.ie, hassan.ali@dit.ie

 

 

Refer to the aspirin production process described in the assignment for module 9001. Prepare a report on the following using a standard referenced report format.

·             Identify and discuss the heat transfer requirements in the aspirin production process.

AND

·             Determine the reactor heat transfer area required which is determined by the cooling required to maintain a reaction temperature of 90 deg cent at start of reaction, assumed to be when reaction temperature reaches 90 deg cent ( CW at 15 deg cent or brine at 0 deg cent available).(reaction rate constant is 5.725 x  10-5 m3 kmol-1 s-1.)

OR

·             Determine the crystalliser heat transfer area.

 

State and justify any assumptions made.

Note: Assume a heat transfer coefficient for vessel of U = 450W m-2 K-1

[20 marks]

 

2. Write a laboratory report in standard format for the ‘Heat transfer/heat exchanger’ experiment (see lab manual for details). A designated period during Semester 1 module 9002 will be set aside to allow collection of data for this experiment.

 

[5 marks]

 

 

Final deadline Jan 5

Draft submissions can be made up to Dec 12 for review and feed back

 

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Module 2 Assignment 2

Fluid Flow

 

Lecturer hassan.ali@dit.ie

 

 

For the production process of aspirin and according to the mass and energy balances that you have performed in Module 9001:

 

1.      Explain and describe methods of fluid transportation between production process units.

 

2.      Acetic anhydride is fed from a storage tank to a batch reactor operating in semi-batch mode for three hours; suggest the complete piping system for this production process unit. Indicate material of construction, pipe sizes, types of pumps, types of valves and flow measurement. This study should also consider pump power required and cost.  State clearly any assumptions you make and reference all information sources used.

 

Note that a defence of your work at interview may be requested to assist in the assessment. The work should be presented in the form of a report using a standard format.

 

[20 marks]

 

 

 

 

Guideline assessment matrix for this assignment

 

%

A

85-100

B

70-84

C

55-69

D

40-54

E

Below 40

 

Theoretical work and or mathematical analysis and solution

 

60

 

Excellent realisation of objectives

Very good realisation of objectives

Good majority of objectives

realised

Fair amount of objectives realised

Fail does not realise objectives

Research

 

30

 

Excellent research of material

Very good research using library and www

 

Some research in library or www

Limited use of references

Has not read up on subject

Standard report format presentation

 

10

 

Excellent presentation

Very good presentation

Good presentation

Fair presentation

Poor presentation

 

 

3. Write a laboratory report in standard format for the ‘Fluid flow’ experiment (see lab manual for details). Tuesday 14th Oct is designated for the lab session period for this experiment in the Chemical Technology Lab Room G 040.

[5 marks]

 

Note:      Final deadline Dec 5

Draft submissions can be made up to Nov.14 for review and feedback

 

 

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