DT275

Module 9003 Assignments

 

 

There are two assignments for this module.  Assignment 1 is a group assignment on Distillation.  The assignment for the Absorption component is a lab session which Hassan will explain to you.

Note that a defence of your work at interview may be requested to assist in the assessment of all assignments.

 

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Module 9003 Assignment 1

Distillation

 

Lecturer gavin.duffy@dit.ie

 

This is a group assignment.  Each group investigates a different binary mixture.  The choice is as follows:

 

Group 1 Ethylene Glycol – Water System

Group 2 Acetic Acid – Acetic Anhydride System

Group 3 Ethanal – Toluene System

Group 4 Ethyl Acetate-Acetic Acid System

 

Assessment

The assessment is broken down as follows:

Individual reflection on project                    40%

Group report                                              30%

Group presentation                                     30%

 

Guideline for the individual reflection on this assignment

For the individual reflection you should:

·        Provide a short summary of what the assignment involved

·        Describe your contribution to the assignment and how you made this

·        Discuss issues that are still not clear to you and provide some possible explanations for these or describe how you would go about resolving these issues

·        You are part of a learning group in this assignment so critically evaluate how your group worked (focus on what you and the others did, i.e. actions, as opposed to who did what, i.e. avoid personality) and provide suggestions for how you could improve.  Use examples to illustrate.

·        Provide some conclusions on this approach to learning

 

Guideline assessment matrix for the report component of this assignment

 

Topic

Max Mark

Adherence to objectives

15

Implementation

(50)

VLE data and graph

10

Mass balance

10

Graphical design

5

Height and diameter

5

Reboiler/condenser

5

Energy Balance

10

Economics

5

Justification of decisions

20

Presentation

15

 

 

Total Mark

100

 

 

Guideline assessment matrix for the presentation component of this assignment

 

Category

Assessment Mark

 

0

1

2

3

4

5

6

7

8

9

10

 

Multiplier

Mark

 

none

poor

fair

good

very good

excellent

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

Quality

 

 

 

 

 

 

 

 

 

 

 

 

x 3 =

 

Communication

 

 

 

 

 

 

 

 

 

 

 

 

x 2 =

 

Understanding

 

 

 

 

 

 

 

 

 

 

 

 

x 5 =

 

(Content, answers to questions, fulfilment of objectives)

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

Total (100)

 

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Module 9003 Assignment 2

Absorption

 

Lecturer ali.hassan@dit.ie

 

 

Part A:   Please answer either problem 1 or 2

 

Problem No. 1 [15 marks]

 

Acetone is to be removed from a 5 per cent v/v acetone-air mixture by scrubbing with water in a packed tower using countercurrent flow. The liquid rate is 0.85 kg/m2s and the gas rate is 0.5 kg/m2s.

The overall absorption coefficient KGa may be taken as 1.5x10-4 kmol/[m3s(kN/m2)], partial pressure difference and the gas-film resistance control the process.

What height of tower is required tower to remove 98% v/v of the acetone? The equilibrium data for the mixture are:

 

Mole fraction acetone in gas:          0.0099      0.0196      0.0361       0.0400

Mole fraction acetone in liquid:  0.0076       0.0156          0.0306       0.0333

 

OR

 

Problem No. 2 [15 marks]

 

A bubble – cap column with 30 plates is to be used to remove n-pentane from solvent by means of steam stripping. The inlet solvent contains 6 kmol of n-pentane /100 kmol of pure solvent and it is desired to reduce the solute content to 0.1 kmol/100 kmol of solvent. Assuming isothermal operation and an overall plate efficiency of 30%, what is the specific steam consumption that is kmol of steam required / kmol of solvent treated, and the ratio of the specific and minimum steam consumptions. How many plates would be required if the ratio is 2.0?

 

The equilibrium relation for the system may be taken as Ye=3.0X, where Ye and X are expressed in mole ratios of pentane in the gas and liquid phases respectively.

 

AND

 

Part B:   Laboratory Practical [10 marks]

 

Details will be provided in class.